The development of Synchrotron X-ray diffraction technique

The application of Synchrotron X-ray diffraction technique 

B.S.   University of Science and Technology of China, Hefei, Department of Polymer Science and Technology, 1995-2000

 Ph.D. Northeastern University, Boston, Department of Chemistry and Chemical Biology, 2000-2006  

   

Research Associate, Brookhaven National Laboratory, New York, Chemistry Department, 2006-2008

Assistant Professor, Shanghai Institute of Applied Physics, Chinese Academy of Sciences, 2008-2009

Associate Professor, Shanghai Institute of Applied Physics, Chinese Academy of Sciences, 2009-2019

Associate Professor, Shanghai Advanced Research Institute, Chinese Academy of Sciences, 2018-2019

Professor, Shanghai Institute of Applied Physics, Chinese Academy of Sciences, 2020-

Professor, Shanghai Advanced Research Institute, Chinese Academy of Sciences,  2020-

Excellent teaching assistant award: 2002-2003, Department of Chemistry and Chemical Biology, Northeastern University

Excellent teaching assistant award: 2003-2004, Department of Chemistry and Chemical Biology, Northeastern University

2nd Place Award, Poster section in National Synchrotron Radiation Facility and Center of Functional Materials Joint Users' Meeting, 2006

First Class Prizes of the State Scientific and Technological Progress Award, 2013

Contribution Award of Shanghai Synchrotron Radiation Facility, Shanghai Institute of Applied Physics, Chinese Academy of Sciences, 2014

   

（1） Self-Assembled-Monolayer-Induced Polyaniline-Grafted Silicon Nanoparticles for Highly Stable Lithium-Ion Battery Anodes, ACS OMEGA, 2025, 第 1 作者
（2） In Situ Formed Amorphous Bismuth Sulfide Cathodes witha Self-Controlled Conversion Storage Mechanism for HighPerformance Hybrid Ion Batteries, Advanced Science, 2024, 
（3） Layered Bismuth Selenide with a Kinetics-Enhanced Iodine Doping Strategy towards High-Performance Aqueous Potassium-Ion Storage, Advanced Functional Materials, 2024, 第 11 作者  通讯作者
（4） Ultrastable Cu2+Intercalation Chemistry Based on a Niobium Sulfide Nanosheet Cathode for Advanced Devices, Acs Nano, 2023, 第 2 作者
（5） Experimental insight into the structure-property relationship and lithium storage mechanism of hydroxyl chloride anchored in the 3D porous conductive matrix, DIAMOND AND RELATED MATERIALS, 2022, 第 9 作者
（6） Stable All-Solid-State Lithium Metal Batteries Enabled by Machine Learning Simulation Designed Halide Electrolytes, NANO LETTERS, 2022, 第 0 作者
（7） Synergistic Engineering of Sulfur Vacancies and Heterointerfaces in Copper Sulfide Anodes for Aqueous Zn-Ion Batteries with Fast Diffusion Kinetics and an Ultralong Lifespan, ADVANCED ENERGY MATERIALS, 2022, 第 15 作者
（8） Identifying Element-Modulated Reactivity and Stability of the High-Voltage Spinel Cathode Materials via In Situ Time-Resolved X-Ray Diffraction, ACS APPLIED MATERIALS & INTERFACES, 2021, 第 7 作者
（9） Structural evolution of mesoporous graphene/LiNi_(1/3)Co_(1/3)Mn_(1/3)O_(2) composite cathode for Li-ion battery, Structural evolution of mesoporous graphene/LiNi1/3Co1/3Mn1/3O2 composite cathode for Li-ion battery, RARE METALS, 2021, 第 11 作者
（10） A stable low-temperature H-2-production catalyst by crowding Pt on alpha-MoC, NATURE, 2021, 第 6 作者
（11） Inconel 617 corrosion in FLiNaK molten salts: An in situ X-ray diffraction study, CORROSION SCIENCE, 2021, 第 11 作者
（12） Facile renewable synthesis of nitrogen/oxygen co-doped graphene-like carbon nanocages as general lithium-ion and potassium-ion battery anodes, CARBON, 2020, 第 10 作者
（13） In Situ Formation of Hierarchical Bismuth Nanodots/Graphene Nanoarchitectures for Ultrahigh-Rate and Durable Potassium-Ion Storage, SMALL, 2020, 第 11 作者
（14） Facile renewable synthesis of nitrogen/oxygen co-doped graphene-like carbon nanocages as general lithium-ion and potassium-ion batteries anode, CARBON, 2020, 第 10 作者
（15） In Situ Studies of 30% Li-Doped Bi 25 FeO 40 ConversionType Lithium Battery Electrodes, ACSOMEGA, 2019, 第 11 作者
（16） Correlating cycle performance improvement and structural alleviation in LiMn 2-x M x O 4 spinel cathode materials: A systematic study on the effects of metal-ion doping, ELECTROCHIMICA ACTA, 2019, 第 6 作者
（17） Carbon-encapsulated niobium carbonitride with high volumetric capacitance and wide potential windows in aqueous pseudocapacitors, ELECTROCHIMICA ACTA, 2019, 第 6 作者
（18） Systematic Study of the Electronic, Carbon, and N-Doping Effects of CoMn-Oxide Composites as Bifunctional Oxygen Electrocatalysts, JOURNAL OF PHYSICAL CHEMISTRY C, 2019, 第 4 作者
（19） A New Intermetallic NiSn5 Phase: Induced Synthesis, Crystal Structure Resolution, and Investigation of Its Mechanism, JOURNAL OF PHYSICAL CHEMISTRY LETTERS, 2019, 第 6 作者
（20） AN IN SITU KINETIC STUDY OF THE DEHYDRATION OF BRUCITE USING SYNCHROTRON X-RAY POWDER DIFFRACTION, CANADIAN MINERALOGIST, 2018, 第 5 作者
（21） Understanding the Strengthening Effect of beta(1) Precipitates in Mg-Nd Using In Situ Synchrotron X-ray Diffraction, JOM, 2018, 第 5 作者
（22） Reconstruction of the Wet Chemical Synthesis Process: The Case of Fe5C2 Nanoparticles, JOURNAL OF PHYSICAL CHEMISTRY C, 2017, 第 6 作者
（23） 混合嗜热古菌在65 ℃生物浸出黄铜矿过程中活性炭的催化作用和钝化现象的相关性, Relatedness between catalytic effect of activated carbon and passivation phenomenon during chalcopyrite bioleaching by mixed thermophilic Archaea culture at 65 ���, TRANSACTIONS OF NONFERROUS METALS SOCIETY OF CHINA, 2017, 第 10 作者
（24） Study of age hardening in a Mg���2.2 wt%Nd alloy by in situ synchrotron X-ray diffraction and mechanical tests, MATERIALS SCIENCE & ENGINEERING A, 2017, 第 5 作者
（25） Facile Construction of Novel 3-Dimensional Graphene/Amorphous Porous Carbon Hybrids with Enhanced Lithium Storage Properties, ACS APPLIED MATERIALS & INTERFACES, 2017, 第 11 作者
（26） An in-situ real time study of the perovskite film micro-structural evolution in a humid environment by using synchrotron based characterization technique, ACTA PHYSICA SINICA, 2017, 第 7 作者
（27） In Situ Monitoring of Structural and Valence Evolution during Electrochemical Desodiation/Sodiation Process of Na2Fe0.5Mn0.5PO4F, JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 2017, 第 5 作者
（28） Great Disparity in Photoluminesence Quantum Yields of Colloidal CsPbBr3 Nanocrystals with Varied Shape: The Effect of Crystal Lattice Strain, JOURNAL OF PHYSICAL CHEMISTRY LETTERS, 2017, 第 8 作者
（29） Study of age hardening in a Mg-2.2 wt%Nd alloy by in situ synchrotron X-ray diffraction and mechanical tests, MATERIALS SCIENCE AND ENGINEERING A-STRUCTURAL MATERIALS PROPERTIES MICROSTRUCTURE AND PROCESSING, 2017, 第 5 作者
（30） Facile usage of a MYTHEN 1K with a Huber 5021 diffractometer and angular calibration in operando experiments, JOURNAL OF APPLIED CRYSTALLOGRAPHY, 2016, 第 11 作者
（31） Influence of Structural Imperfection on Electrochemical Behavior of Prussian Blue Cathode Materials for Sodium Ion Batteries, JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 2016, 第 5 作者
（32） Exploring the working mechanism of Li+ in O3-type NaLi0.1Ni0.35Mn0.55O2 cathode materials for rechargeable Na-ion batteries, JOURNAL OF MATERIALS CHEMISTRY A, 2016, 第 6 作者
（33） Effect of direct current pulses on mechanical and electrical properties of aged Cu���Cr���Zr alloys, MATERIALS & DESIGN, 2016, 第 5 作者
（34） 嗜酸热古菌Acidianus manzaensis浸出黄铜矿过程中次生矿物的形成及演变, Formation and evolution of secondary minerals during bioleaching of chalcopyrite by thermoacidophilic Archaea Acidianus manzaensis, 中国有色金属学报：英文版, 2016, 第 4 作者
（35） A lithiation/delithiation mechanism of monodispersed MSn5 (M = Fe, Co and FeCo) nanospheres, JOURNAL OF MATERIALS CHEMISTRY A, 2015, 第 4 作者
（36） Introduction of the X-ray diffraction beamline of SSRF, NUCLEAR SCIENCE AND TECHNIQUES, 2015, 第 2 作者
（37） epsilon-Iron carbide as a low-temperature Fischer-Tropsch synthesis catalyst, NATURE COMMUNICATIONS, 2014, 第 4 作者
（38） Strain Induced Metastable Phase and Phase Revolution in PbTiO_3-CoFe_2O_4 Nanocomposite Film, CHINESE PHYSICS LETTERS, 2014, 第 6 作者
（39） Comparative investigation on the properties of carbon-supported cobalt-polypyrrole pyrolyzed at various conditions as electrocatalyst towards oxygen reduction reaction, INTERNATIONAL JOURNAL OF HYDROGEN ENERGY, 2014, 第 6 作者
（40） Local structures around 3d metal dopants in topological insulator Bi2Se3 studied by EXAFS measurements, PHYSICAL REVIEW B, 2014, 第 0 作者
（41） Surface modified cfx cathode material for ultrafast discharge and high energy density, JOURNAL OF MATERIALS CHEMISTRY A, 2014, 第 6 作者
（42） Corrigendum to "Toward high capacity and stable manganese-spinel electrode materials: A case study of Ti-substituted system" J. Power Sources 245 (2014) 570���578, JOURNAL OF POWER SOURCES, 2014, 第 6 作者
（43） Toward high capacity and stable manganese-spinel electrode materials: A case study of Ti-substituted system, JOURNAL OF POWER SOURCES, 2014, 第 6 作者
（44） Oxygen Reduction Contributing to Charge Transfer during the First Discharge of the CeO2-Bi2Fe4O9-Li Battery: In Situ X-ray Diffraction and X-ray Absorption Near-Edge Structure Investigation, JOURNAL OF PHYSICAL CHEMISTRY C, 2014, 第 11 作者
（45） Graphene/Au composite paper as flexible current collector to improve electrochemical performances of CFx cathode, JOURNAL OF POWER SOURCES, 2014, 第 5 作者
（46） Toward high capacity and stable manganese-spinel electrode materials: A case study of Ti-substituted system (vol 245, pg 570, 2014), JOURNAL OF POWER SOURCES, 2014, 第 6 作者
（47） Structure of Clusters and Formation of Amorphous Calcium Phosphate and Hydroxyapatite: From the Perspective of Coordination Chemistry, CRYSTAL GROWTH & DESIGN, 2013, 第 8 作者
（48） Effects of cobalt precursor on pyrolyzed carbon-supported cobalt-polypyrrole as electrocatalyst toward oxygen reduction reaction, NANOSCALE RESEARCH LETTERS, 2013, 第 7 作者
（49） A "Smart" Hollandite DeNOx Catalyst: Self-Protection against Alkali Poisoning, ANGEWANDTE CHEMIE-INTERNATIONAL EDITION, 2013, 第 3 作者
（50） Understanding the High Capacity of Li2FeSiO4: In Situ XRD/XANES Study Combined with First-Principles Calculations, CHEMISTRY OF MATERIALS, 2013, 第 6 作者
（51） 电化学原位同步辐射技术在锂离子电池电极材料研究中的应用, 电化学, 2013, 第 5 作者
（52） Effects of Pyrrole Polymerizing Oxidant on the Properties of Pyrolysed Carbon-Supported Cobalt-Polypyrrole as Electrocatalysts for Oxygen Reduction Reaction, JOURNAL OF THE ELECTROCHEMICAL SOCIETY, 2013, 第 5 作者
（53） Synthesis, characterization and luminescent properties of needle-like lanthanide-doped orthorhombic Y5O4F7, JOURNAL OF RARE EARTHS, 2013, 第 7 作者
（54） Periodic elastic nanodomains in ultrathin tetragonal-like BiFeO3 films, PHYSICAL REVIEW B, 2013, 第 0 作者
（55） The Structure-Property Investigation of Bi1-xCexFeO3 (x=0, 0.05)-Li Battery: In Situ XRD and XANES Studies, JOURNAL OF PHYSICAL CHEMISTRY C, 2012, 第 11 作者
（56） 锂离子电池正极材料Na3V2（PO4）2F3的原位XRD及固体核磁共振研究, In situ XRD and solid state NMR characterization of Na3V2(PO4)2F3 as cathode material for lithium-ion batteries, 中国科学：化学, 2012, 第 4 作者
（57） SR-XRD和EXAFS研究Mn掺杂ZnO薄膜的微观结构, SR-XRD and EXAFS study on microstructure of Mn doped ZnO films, 核技术, 2012, 第 7 作者
（58） Electrochemical characteristics and intercalation mechanism of ZnS/C composite as anode active material for lithium-ion batteries, ELECTROCHIMICA ACTA, 2011, 第 5 作者
（59） Facile solid-phase synthesis of the diammoniate of diborane and its thermal decomposition behavior, PHYSICAL CHEMISTRY CHEMICAL PHYSICS, 2011, 第 6 作者
（60） A novel Li2FeSiO4/C composite: Synthesis, characterization and high storage capacity, JOURNAL OF MATERIALS CHEMISTRY, 2011, 第 2 作者
（61） BiFeO3 as Electrode Material for Lithium Batteries, JOURNAL OF NEW MATERIALS FOR ELECTROCHEMICAL SYSTEMS, 2011, 第 11 作者
（62） Thermal phase transformation of In2Se3 nanowires studied by in situ synchrotron radiation X-ray diffraction, JOURNAL OF MATERIALS CHEMISTRY, 2011, 第 8 作者
（63） The quantitative monitoring of mechanochemical reaction between solid l-tartaric acid and sodium carbonate monohydrate by terahertz spectroscopy, JOURNAL OF PHYSICS AND CHEMISTRY OF SOLIDS, 2011, 第 7 作者
（64） 上海光源在材料与能源科学中的应用, 现代物理知识, 2010, 第 2 作者
（65） In Situ Characterization of CuFe2O4 and Cu/Fe3O4 Water-Gas Shift Catalysts, JOURNAL OF PHYSICAL CHEMISTRY C, 2009, 第 6 作者

1) Lithium battery apparatus for synchrotron X-ray diffraction investigation, 2012

2) Synchrotron radiation based nano materials growth aparatus, 2012

3) Aparatus for facile adjustment of Mythen 1K Si based linear detector, 2016

Development of Synchrotron Radiation X-ray diffraction techniques

Application of  Synchrotron Radiation X-ray diffraction techniques

（1）Operando Structure-property Studies of Bismuth Based Oxygen Ionic Conductors for Lithium Batteries Applications    2019国际电化学能源系统大会   2019-03-26
（2）上海光源衍射线站介绍   第一届全国同步辐射表征方法在电池领域应用前沿研讨会   2018-12-19
（3）Introduction of Shanghai Synchrotron Radiation Facility   2018-11-21
（4）In Operando Structure-property Studies of Advanced Nano Materials for Lithium Batteries   第9次亚太同步辐射论坛暨澳大利亚同步光源用户年会   2015-11-24
（5）Current Lithium Ion Battery Research Using Shanghai Synchrotron Radiation Facility (SSRF)    Wen Wen, Mei Gao, Xingmin Zhang, Yueliang Gu, Guangzhi Yin, Tieying Yang, Xingyu Gao    2014-03-13
（6）Bismuth Ferrites as Electrodes for Lithium batteries: An in situ XRD and XANES Investigation   224 次电化学会会议   Wen Wen, Min Liu, Chuan Lin, Yueliang Gu, Tieying Yang, Zhengliang Gong, Guangzhi Yin, Xingyua Gao, Xingtai Zhou   2013-10-27
（7）上海光源以及目前在锂电池上的应用    第三十次全国化学与物理电源学术年会   文 闻, 顾月良，阴广志，杨铁莹，龚正良，高兴宇    2013-07-12

与国内外锂电池用户研究专家展开合作，对于多种体系进行研究，并有多篇成果获得发表。

1）李景坤，杨轲，文闻，陆美凤，马紫峰，高电位LiNi0.5Mn1.5O4正极材料制备、电化学性能与结构相变，储能科学与技术，2016，5。

2）Xin, F. X.，Wang, X. L.，Bai, J. M.，Wen, W.,Tian, H. J.，Wang, C. S.，Han, W. Q., 单分散 MSn5(M=Fe,Co以及FeCo)纳米球的嵌锂/脱锂机理，Journal of Materials Chemistry A，2015，3（13）：7170-7178。

3）Dai, Y. ，Cai, S. D.，Wu, L. J.，Yang, W. J.，Xie, J. Y. ， Wen, W.，Zheng, J. C.，Zhu, Y. M.，超快放电以及高能量密度的表面修饰CFx阴极材料，Journal of Materials Chemistry A，2014，2（48）：20896-20901。

4）龚正良，张炜，吕东平，郝晓罡，文闻，姜政，杨勇，电化学原位同步辐射技术在锂离子电池电极材料研究中的应用，电化学，2013，（06）：512-522。

5）郝小罡，刘子庚，龚正良，文闻，谈时，杨勇，锂离子电池正极材料Na3V2(PO4)2F3的原位XRD及固体核磁共振研究，中国科学:化学，2012，（01）：38-46。

6）Zhong, K. F.，Zhang, B.，Luo, S. H.，Wen, W.，Li, H.，Huang, X. J.，Chen, L. Q.，多孔MnO 微球锂离子电池阳极材料研究，Journal of Power Sources，2011，196（16）：6802-6808。

现指导学生

张逸浩  硕士研究生  085400-电子信息